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CasNo: 69260-42-0
MF: C14H16O5
PURPOSE: A photosensitive polymer prepar...
The present invention relates to a novel...
This invention provides a chemical compo...
The synthesis and phase behavior of thre...

4-(ω-hydroxybutoxy)benzoic acid


acryloyl chloride

![4-[(4-propenoyloxy)butyloxy]benzoic acid](/upload/2024/7/7b689aa0-83c9-43be-bcd7-14d736a8a919.png)
4-[(4-propenoyloxy)butyloxy]benzoic acid
| Conditions | Yield |
|---|---|
|
With N,N-dimethyl-aniline; In N,N-dimethyl acetamide; at 0 - 20 ℃; Inert atmosphere;
|
|
|
With dmap; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;
|
33 g |
|
4-(ω-hydroxybutoxy)benzoic acid; With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;
acryloyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 25h;
|

4-(ω-hydroxybutoxy)benzoic acid


acrylic acid

![4-[(4-propenoyloxy)butyloxy]benzoic acid](/upload/2024/7/7b689aa0-83c9-43be-bcd7-14d736a8a919.png)
4-[(4-propenoyloxy)butyloxy]benzoic acid
| Conditions | Yield |
|---|---|
|
With toluene-4-sulfonic acid; hydroquinone; In chloroform; Dean-Stark; Reflux;
|
65% |

4-(ω-hydroxybutoxy)benzoic acid

acrylic acid

acryloyl chloride

Ethyl 4-hydroxybenzoate

2-methyl-1,4-phenylene bis(4-(4-(acryloyloxy)butoxy)-benzoate)